By H. Miyamoto, M. Salomon

ISBN-10: 0080292100

ISBN-13: 9780080292106

This quantity provides compilations and important reviews of pronounced solubility facts for the name compounds released as much as mid-1984. those compounds have an incredible position within the historical past of analytical chemistry; sensible functions comprise their use in pyrotechnics and the paper pulp undefined. additionally incorporated are uncomplicated computing device courses which enable the calculation of solubilities at any temperature

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Extra info for Alkali Metal Halates, Ammonium Iodate & Iodic Acid

Sample text

FiJUg. 0 0. 5 1. 0 2. 1 4. ,5 99. 0 97. ,0 100 97. 5 95. 2 89. 0 86. 6 82. 3 80. 9 80. 5 79. 5 79. 7 77. 4 72. 6 75. 6 69. 9 69. 3 66. 2 61. 3 continued AUXILIARY INFORMATION METHOD/APPARATUS/PROCEDURE : SOURCE AND PURITY OF MATERIALS: Two different methods were used to deterNo information was given. mine the solubility of lithium chlorate in water. (1) Synthetic method used with visual observation of temperature of crystalization. The weighed salt and water were placed into a test-tube equipped with a stirrer and a thermocouple.

1923, 123, 2712-3. C. 16 Nature of the solid phase not specified. AUXILIARY INFORMATION SOURCE AND PURITY OF MATERIALS: METHOD/APPARATUS/PROCEDURE : Nothing specified. A solution of sodium chlorate, saturated at the boiling point, was stirred vigorously in an electrically controlled thermostat at the required temperature for about three hours. A weighed sample was evaporated in a conical flask by immersing this in a bath at 100°C and gently distilling benzene on to the surface of the liquid. In about fifteen minutes the salt was obtained in a thin crust over the bottom of the flask.

To remove the last trace of water, the salt was placed in a vacuum oven over phosphorus pentoxide , and maintained at 80°C. 4 % (authors) Temp: precision ± 0 . 0 5 Κ (authors). Thermal analysis : nothing specified. E. [7447-41-8] [13453-71-9] Can. J. Chw. 1956, 34, 1647-61. 15. 2 continued AUXILIARY INFORMATION METHOD/APPARATUS/PROCEDURE : The isothermal method was used. Equilibrium was approached from two directions. A given solution was divided into equal parts, and one part was heated to complete disolution of the solid, and the second part was completely frozen.

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Alkali Metal Halates, Ammonium Iodate & Iodic Acid by H. Miyamoto, M. Salomon

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